专利摘要:
The present invention removes toxic substances or harmful bacteria in the body during digestion to prevent food poisoning, promote digestion to maintain health and restore the normal human function edible charcoal using pine charcoal for use as the main raw material of health food ( Regarding the manufacturing method of Charcoal), The manufacturing process of the present invention is mixed with 90% by weight of red pine or Korean native pine charcoal (Charcoal) and 10% by weight of salt (Salt) in the blast furnace, the door is closed and then edible having a very small pores through a high temperature treatment of 600 ℃ It is characterized in that it is prepared as a charcoal and pulverized with 325 mesh and mixed with 10% by weight of aloe powder to 90% by weight of the edible charcoal to prepare it as a main ingredient of health food, The present invention is used as a main raw material of health food is to remove toxic components or harmful bacteria in the body during digestion to prevent food poisoning, promote digestion to maintain health and restore the normal function of the human body.
公开号:KR20020093432A
申请号:KR1020010032187
申请日:2001-06-08
公开日:2002-12-16
发明作者:차순옥
申请人:차순옥;
IPC主号:
专利说明:

The manufacturing process of edible charcoal using pine charcoal}
[1] The present invention removes toxic substances or harmful bacteria in the body during digestion to prevent food poisoning, promote digestion to maintain health and restore the normal human function edible charcoal using pine charcoal for use as the main raw material of health food ( Charcoal).
[2] Although charcoal has excellent adsorptive power, its raw material is made of oak or mixed scrub, and its permeability is strong, so that its components may remain in the human body and impurities remain, which is unsuitable for food.
[3] The present inventors have been studying charcoal material for 20 years, and Korean native pine tree can be crushed into 325mesh, which is adaptable to human body, is mild and fragrant, and is the best technology of powder, and there is no negative factor, so it is the charcoal raw material of the present invention and salt (Salt) ), Because it removes impurities at high temperature and is good for human adaptation, the salt is mixed with charcoal in the blast furnace and processed into charcoal CHA12 which has very small pores through high temperature treatment of 600 ℃, then cooled and crushed into powder of 325 mesh. It has been successful in manufacturing food carbon, the main ingredient of health food supplements for patients.
[4] Edible carbon prepared by the present invention has an excellent effect of adsorption and detoxification of various toxic substances, pesticides, environmentally harmful substances, harmful bacteria, wastes, etc., which are harmful to the human body,
[5] At this time, the substances beneficial to the human body do not adsorb the harmful substances and then act safely to be excreted.
[6] Recently, vegetables, fruits, bean sprouts, etc. can not be eaten freely, and meat, fish, eggs, etc. are changing freely. Once upon a time, an egg went bad in three days. But now, no matter how many months you leave. Eggs should go bad after three days. There are reasons why the bread will not rot after three days. Too many antibiotics and preservatives are traced in eggs or bread. It is an age when the living environment is changed to the bad side at a frightening speed and water cannot be drunk at will. Imported feedstock has been embalmed during the import process and the outer skin is used as feedstock. And when the feed is prepared by mixing antibiotics, nutrients and the like. Almost all of the toxins are transferred to meat or fish and to meat eaters.
[7] The times are changing and the environment is changing, and the disease that is not cured by medicine due to the environment and tolerance is increasing day by day. Diseases that cannot be cured by drugs such as trauma and various skin diseases are increasing exponentially. The reason is that there are toxic substances, environmental substances, or strong bacteria in the infected area. Man or animal or ten o'clock. We always eat pesticides, toxic substances, environmental substances and bacteria through fruits, vegetables, grains and foods. This is the source of all illnesses. Cancer, various diseases, skin diseases, inflammation, high blood pressure, nervous system diseases, digestive diseases, modern diseases, dementia, etc.
[8] Vegetable and fruit growers spray pesticides today and ship them to the market tomorrow. If pesticides enter the body, it is fatal. Pesticides are fatal to the liver. If these pesticides remain in the liver or ducts for a long time, hepatitis or cirrhosis and cancer may occur. The small amount that enters the body is irrelevant because the liver is processed, but if it continues to enter, the toxic components that are not processed by the liver primarily cause disorders in the digestive system and spread through the blood vessels throughout the body. Then all functions are impaired. Almost all diseases today are not cured by medicine. Many people lose important lives by not being able to get rid of toxics.
[9] 1. There is no limit to list the fatal problems that occur when various toxic substances or harmful substances enter the body.
[10] One). Liver disease such as alcoholism, cirrhosis, liver cancer
[11] Toxic substances of the liver are toxic.
[12] When alcohol or toxic substances enter the body, they are sent to the liver for decomposition. If this happens over and over, the liver cells are permanently damaged. In an effort to treat this damage, scar tissue forms on the surface of the liver. This tissue is covered with hard nodules throughout the liver as well as the surface of the liver. The liver is then enlarged, hardened and covered with nodules. The disease is called cirrhosis. Afterwards, important complications usually come and this worsens the condition. One in five cirrhosis patients develops liver cancer. It also develops into liver tumors. It may be the first sign of liver cancer. The second is toxins that penetrate the body. If this toxin continues to enter, it harms the liver and later develops into cirrhosis. The liver, gallbladder, and pancreas are the source of the disease. Many diseases start here. The liver is the invasion zone or cancer metastasis zone of the second cancer.
[13] When you drink alcohol, too much alcohol is absorbed into your blood or body via your liver. At this time, the liver filters out bad substances and harmful alcohol. By 10-20 years, the liver cannot function and the unfiltered alcohol spreads throughout the body and becomes addicted. Liver cirrhosis is a progressive chronic inflammation of the liver, typically caused by chronic alcoholism or severe chronic hepatitis.
[14] 2). Causes of Other Cancers
[15] In the old days, there was not much cancer.
[16] They have only lost many lives due to epidemics and bacteria living in unclean places. Why do so many cancers happen now
[17] Stomach cancer, lung cancer, esophageal cancer, breast cancer, uterine cancer, blood cancer and other unknown cancers are occurring and widespread. Why What is the cause
[18] Statistics show that more than 98% of cancers occur after age 40. Uterine cancer is more than 40 years old, lung cancer is 45-65 years old, gastric cancer, rectal cancer, colon cancer is 45-50 years old. Nearly all cancers occur more than 45 years old. Why
[19] Why does it rarely cause cancer to age under 45 What is the reason
[20] Under 45 years old, they are not freed from cancer, but rather develop cancer. I just can't find it. Cancer is not a disease you get overnight. For at least 10 years, some causes accumulate and become weaker, leading to cancer. In lung cancer, more than 98% of lung cancers are between 45 and 65 years old. He is older than other cancers. Smokers, as well as miners in uranium mines, workers in nickel smelting plants, workers in chromate and asbestos plants, and workers in coal cutlet plants are very likely to develop lung cancer. And it usually takes 30 years to develop lung cancer. Why This is because toxic substances continue to enter the lungs and remain in the lungs for a long time. Once toxic components remain, some toxic components last a lifetime. There is no way for Hyundai to be free from toxicants. Toxins are present in vegetables, sprouts, fruits, grains, meat, and the environment, and they are introduced into the body. Small amount of preservative does not matter. So there is a tolerance. But what happens if you keep in your body If you keep going for 1, 2, 10 years, you first weaken the liver function, harm the lungs and weaken the five senses. If poison or harmful substances enter the body to the liver, liver function is limited. When the liver's function is weakened, poison or harmful substances spread in the body. The poisonous area is surrounded by fluid, which later becomes inflamed and ages as a cause of cancer. There is no medicine to deal with this toxic component. Inflammation or cancer develops toxins as the inflammation or cancer develops. Strong drugs are used in the treatment process and there are toxins in the strong drugs. Daily elimination of these toxins is fundamental to treating inflammation or cancer. In the past, in no case did poison enter the body. It is gradually revealed that the cause of modern hospitals is the accumulation of toxins. The best way to stay healthy is to get rid of the toxins in your body. CHA12 strongly adsorbs and detoxifies toxic and harmful bacteria in the body.
[21] 2. The effects of CHA12 on diseases caused by toxic substances, harmful substances, harmful bacteria, and waste products are as follows.
[22] One). Amazing Toxin Adsorption
[23] 1 g of CHA12 adsorbs 1500 to 3000 mg of toxic components. In addition, the amount of ammonia gas 200 is adsorbed to the amount of CHA12 1. As such, the amount of adsorption varies depending on the type of gas or drug, and the adsorption varies depending on the physical and chemical properties, that is, the ionization state and the molecular weight. CHA12 is porous and the more finer it is, the more powerful it is. CHA12 is pulverized with 325Mesh, the best technology of pulverization, and it removes all the irritating surface to maximize the adsorption in the body. Physical adsorption to CHA12 occurs in all compounds, but chemical adsorption may occur in part depending on the type of compound. In other words, CHA12 poisonous adsorption is largely reversible. This CHA12 absorbs toxins from the intestine. Adsorption increases the clearance of drugs that have already been absorbed, which significantly reduces the biological half-life (which reduces the effectiveness of the drug in half). For example, the sleeping pills phenobalbital are reduced from 110 hours to 19.8 hours, and theophylline for bronchial asthma is reduced from 6.4 to 3.3 hours, and the heart disease digoxin and digitoxin are reduced from 23 to 17 hours and 110 to 51 hours. . The drugs we eat are absorbed in the intestine or stomach, into the blood and spread throughout the body, mainly broken down by the liver. CHA12 not only prevents oral medications from being absorbed into the blood, but also reduces blood vessels. In other words, the absorbed drug is returned to the intestine and is resorbed by CHA12 in the intestine. That is, the more CHA12 the drug enters the intestine from the blood by various methods, the more likely this happens. The concentration of the drug diffused into the intestine is reduced to almost zero. In other words, it prevents backflow into the blood. In addition, the drug escaped through the liver is also adsorbed. The removal of poison or drugs through the intestine is called gastrointestinal dialysis. The method of directly removing the poison in the blood using CHA12 is called blood perfusion. And peritoneal dialysis is a method of removing drugs or poisons through the peritoneum, of which gastrointestinal dialysis is the most effective.
[24] 2). Draft effect
[25] This CHA12 is a poisonous bacterium, as well as detoxification and medicine. It also removes viruses, carbon dioxide and hydrogen. That is, 1g adsorbs 50cc of carbon dioxide and 3cc of hydrogen. As described above, the larger the attraction force is, the better the adsorption is caused by the mutual attraction between molecules. These adsorbed drugs and poisons include mental illness drugs (stimulants, sleeping pills, sedatives), neuralgia drugs, heart disease drugs, alkaloids (caffeine, morphine, nicotine, etc.), antihistamines, analgesics, antipyretics, antibiotics, allergens, Radioactive materials, carcinogens, pesticides, and arsenic materials. Of course, there is a difference in the degree of adsorption according to the experiment. However, inorganic substances (hydrochloric acid, iron, cyan salt), DDT and the like do not adsorb. If the drug is taken too much for an emergency, or if it is unconscious because the time is too long, even if the drug is well adsorbed and removed by CHA12, vomiting it first, and if it is unconscious, after gastrointestinal lavage and administration, good. To increase the effectiveness of CHA12, wash the stomach as soon as possible and administer a large amount of CHA12 immediately. CHA12 has a wide safety range (between effective and lethal doses) and few side effects and contraindications. That is, it is the best as a single administration substance for detoxification. Efficacy depends on the dose, the method of administration, the time of administration, and the presence or absence of food in the stomach and should be eaten as soon as possible. It takes nine months to get rid of congenital jaundice, which causes more than 90% drop in activity without side effects. No problems have been reported with the liver, kidneys, and hematopoietic organs. Pesticides, herbicides, etc. can be used to remove poisons accumulated in the body for a long time, and also to remove intestinal bacteria such as diarrhea and indigestion. It can be taken at the same time as a bee or snake bite at the same time as my surgical treatment, or to remove cholesterol.
[26] 3). Hyperlipidemia treatment effect
[27] Cholesterol consists of low density lipid protein and high density lipid protein, many of which are mainly low density lipid protein. In other words, healthy people have a good balance between dietary cholesterol and cholesterol produced by the body. Soon, as dietary cholesterol increases, the body's cholesterol decreases, and the body defends itself from increasing cholesterol levels. Dietary cholesterol is absorbed by the intestine, increasing the concentration of low-density lipid proteins in the blood, and is also used by the body for cholesterol. It can also cause coronary artery disease and high blood pressure. In the experiment, administration of CHA12 to hypercholesterolemia decreased the concentration of low density lipid protein and increased the concentration of high density lipid protein. The hyperlipidemic effect is no less than the effect of cholestyramine, a serum lipid-lowering drug. First in terms of safety. CHA12 also slightly reduces blood pressure. When CHA12 was administered, there were no changes in blood components other than lipid changes, which makes it suitable as a drug or a therapeutic aid. It adsorbs the toxic components in the bile that enters the 12 jang through the intestinal circulation and adsorbs the toxic components in the metabolites.
[28] As described above, the CHA12 material of the present invention becomes a main ingredient of patient-specific treatment aid by strongly adsorbing and detoxifying and recovering human function and toxic substances, pesticides, environmentally harmful substances, harmful bacteria, and waste products that cause modern diseases. .
[29] * Toxic and gastric ulcers, gastric cancer, colon cancer, rectal cancer, stomach, large intestine, 12 diseases of the colon
[30] The length of the intestine is generally 8-10 m and the transit time is 20-50 hours. The longer the transit time, the higher the incidence of bowel disease, which later affects the entire human body. The longer the passage, the longer the toxins from the food during the passage of the intestines. Carcinogens, toxins, or irritants can continue to irritate the inside of the colon, causing colon cancer. The solution to this is simple. You can get rid of toxins from eating and eating fiber foods. If the stomach and intestines are comfortable, the whole human body is comfortable.
[31] 1. The stomach and duodenum are very important parts of the human digestive system. After the pyloric value in the stomach, the duodenum is next. Toxic substances and incisions can cause adverse reactions and ulcers. It can also cause inflammation of the entire stomach wall. Gastric cancer, one of the most deadly forms of cancer, also occurs here. The stomach is one of the most common cancer sites. Ulcers occur more often than among patients on medication.
[32] * Above: Toxins such as alcohol and molpin are well absorbed. Food mixes well with gastric juice to become semifluid-chyme, which is sent to the duodenum by peristaltic movement.
[33] * Nausea and nausea: Excessive kidney and / or intestinal toxicity. Toxic. Excessive alcohol. Irritating foods, drugs, and toxic substances are the causes of nausea and vomiting.
[34] 2. Small and large intestine
[35] * Small intestine: divided into duodenum, jejunum and ileum, the juice from the stomach is mixed with bile juice produced by the liver and pancreatic juice secreted by the pancreas and digested. It absorbs nutrients while passing through the small intestine. The liver and gallbladder are appendages to the small intestine. Bile is produced in the liver and discharged into the duodenum.
[36] * Colon: Absorbs moisture from food waste from the chairman to make feces, semi-solids, accumulate for a certain period of time, and defecate. Feces are food waste, dropped epithelial cells, leukocytes, bacterial stomach and intestines, and liver and pancreas secretions. Collected in the colon by mixing movement, peristaltic movement and defecation through the rectum.
[37] Gastrocolic reflex: After eating, the mass contraction starts from the caecum and sweeps the colon, pushing it into the sigmoid colon or rectum. Some may be stagnant in the sigmoid colon for three days before going back to work. When stagnant, toxic components can cause gastrointestinal reflex problems.
[38] 3. Diseases
[39] Food poisoning: Caused by infection with Salmonella or Shigella that invade the barrier. Salmorella invades the enterocytes against the microthorax. Typhoid is infected by Salmonella.
[40] Malnutrition absorption: caused by factors that prevent bile or pancreatic fluid from entering the small intestine, damage the intestinal mucosa (severe bacterial infection and neomycin treatment), or reduce the surface area of absorption.
[41] Gastric ulcer: When the mucosal barrier is destroyed, it causes inflammation of the stomach wall. Persistent damage to tissues causes gastric ulcers. The causes of gastric ulcers are over-hydrochloric acid and under-secretion of mucus. Aspirin and NSAIDs (nonsteroidal anti-inflammatory druge) Smoking, drinking, coffee and stress affect mucus production and toxic compounds impair its function. Fat soluble substances such as alcohol, aspirin and toxic components easily pass through the gastric mucosa into the blood.
[42] Gastric cancer: The body of stomach cancer is not clearly identified. Stomach cancer is a very common disease and causes the most cancer deaths in men. 98% of patients appear in people over 45 years old. We need to see why stomach cancer appears in people over 45 years old. It can be seen that some of the factors occur in the continuous process. Stomach ulcers are one of the major causes of gastric ulcers. The causes of gastric ulcers can be attributed to toxic substances or bacteria such as inflammation of the stomach wall, smoking (nicotine), alcohol (alcohol) coffee (cocaine) as described above.
[43] * Bowel Cancer, Colon Cancer, Rectal Cancer
[44] Like gastric cancer, it occurs in people over 45 years of age, and the cause is very similar. Alcohol and toxic components remain during digestion, intestinal circulation, gastrointestinal reflex, mixed movement, interlocking movement, digestion to defecation and cause all diseases.
[45] Peam
[46] One). Causes of the development of lung cancer
[47] Smoking is the most important cause of lung cancer known to us. Smoking is directly related to the number of cigarettes (price's text book of the practice of medicine states) .The mortality rate of tobacco-heavy bones is 20 times higher than those who do not smoke. Until the diagnosis is confirmed as lung cancer, cancer cells usually spread through the bloodstream or lymph nodes to distant parts of the body. There is no part where cancer cells do not spread. At this point it is hopeless.
[48] 2). If you look at lung cancer
[49] More than 98% of lung cancers are between 45 and 65 years old. Age is higher than other cancers. Smokers, as well as miners in uranium mines, workers in nickel smelting plants, workers in chromate and asbestos plants, and workers in coal cutlet plants are very likely to develop lung cancer. And it usually takes 30 years to develop lung cancer. Why is that Nicotine continues to enter the lungs, harming the lungs for a long time and eventually causing lung cancer.
[50] 3). Smoking and heart disease
[51] Smoking is the cause of coronary artery infarction and many other cardiovascular diseases. Many experts now say smoking is by far the single cause of heart disease. Among the causes of death in the West, heart disease and cardiovascular disease play a leading role, accounting for over 50% of all deaths.
[52] The harmful effects of smoking on the heart and blood vessels are far more dangerous than you think. In practical terms, one in three male deaths between the ages of 35 and 64 dies from coronary heart disease. And one in seven women of the same age die from the disease. Smokers are twice as likely to get heart disease as nonsmokers. And it has to do with the amount of cigarettes smoked, the amount of smoke you breathe in, and the age at which you start smoking. After quitting, the risk for the disease gradually decreases.
[53] * Pregnancy and tobacco
[54] Babies who smoke among pregnant women are born on average 150-240g lighter than babies. The weight of newborns is important because babies with lower weights have a much higher mortality rate at birth than babies of normal weight.
[55] * Nicozin and oropharyngeal cancer of the larynx
[56] Several studies conducted by the Royal College of Medicine in London indicated that oral cavity, pharyngeal larynx, and esophageal cancer were associated with smoking in cigarettes, pipe tobacco, or cigars, and provided supporting evidence. In recent years, the risk of bladder cancer has increased in smokers, and the number of frequently recurring latent diseases is increasing. Smoking is also a very bad cause of dyspnea. It is certain to retard the treatment of peptic ulcers. Some research in the United States shows that the number of people who die from peptic ulcers is largely smokers.
[57] * Nicotine and hearing
[58] Dr. Nikanishi, a well-known Japanese doctor whose hearing loss was higher as he smoked, conducted a hearing test on 15,54-year-old males aged 30-59 years from 1994 to 1999. The amount of hearing was found to drop. Those who smoked one pack a day for more than 10 years were three times more likely to have a hearing loss than nonsmokers. Smokers are at high risk for hearing damage because smoking reduces the blood flow to the cochlea, a snail-like region of the inner ear that transmits sound to the brain.
[59] Toxic components, mental illness and drug addiction
[60] Mental illness (stimulants, sleep, sedatives)
[61] It is closely related to liver and mental illness. In the treatment of mental illness, stimulants, sleeping pills, and sedatives continue to be administered. These treatments spread throughout the blood vessels throughout the body, leaving serious sequelae. Accumulation of these components can cause serious damage to the human body and, rather than treatment, most of the mental disease worsens. These drugs should be prevented from entering the bloodstream and the accumulated toxins should be removed. Liver function should also be restored. The same is true for drug addicts.
[62] * Toxic and Gynecological Diseases
[63] There were very few uterine or breast cancers on that day. Breast cancer is now a very common disease among women living in the West, but its incidence continues to increase. The incidence of uterine cancer and breast cancer is higher in cities than in the countryside and far higher in the West than in the East. The sad fact is that breast cancer mortality rates have not declined significantly over the last 50 years, despite the mobilization of various institutions, support and modern technology.
[64] Uterine cancer and breast cancer
[65] The most vulnerable part of a woman's reproductive system to cancer attack is the cervix. More than 60% of uterine cancers occur in the cervix. It is estimated that 2 out of 100 women will develop cervical cancer. The next most vulnerable part of a woman's body to cancer is the breast.
[66] * Causes of breast cancer: (1) Early menopause and late menopause
[67] (2) If you have never experienced pregnancy or are pregnant late
[68] (3) X-ray overexposed
[69] (4) smoking and excessive alcohol intake
[70] (5) Notice
[71] (6) old age
[72] (7) breast cancer and strength
[73] (8) Family history of breast cancer
[74] (9) Toxic substances that enter the body through several oils.
[75] Toxic and Obese
[76] Obesity is a national problem in the West. As the western world thrives and develops, so does the weight of the people. Half of the world is dying of hunger, while the other half is dying of eating. Literally, their teeth are digging their graves. Obesity causes serious and many diseases. Heart disease and heart attack are common in people who are obese. The same applies to arteriosclerosis, arthritis, diseases of the joints, diabetes, gallbladder, liver disease, hypertension, and gout. Pregnancy also interferes with growth and slows fertility. part
[77] The state is also a serious problem in national management. The longer the belt, the shorter the lifeline. Losing weight is a lifelong task.
[78] ① If a person is over 12Kg, it is like living with the same weight of rock for a lifetime. Activity is degraded.
[79] Due to the heavy weight, the body's activity is slow, the head is dull, and the movement and behavior are not active.
[80] ③ When the body's fat metabolism occurs, cholesterol in the blood increases and the sinus is hardened. Therefore, the blood pressure rises and the headache, scalp, snarl, and shoulders feel stiff.
[81] ④ When a metabolic disorder occurs, other metabolisms related to this disorder are also affected, and diabetes, arthritis, etc. appear.
[82] cholesterol in the coronary arteries of the heart, hardening occurs, angina, myocardial infarction, heart failure is likely to occur.
[83] cholesterol in the gallbladder accumulates, gallstones are likely to occur.
[84] gastrointestinal symptoms, constipation tends to appear and is prone to hemorrhoids.
[85] Men have decreased output and women have reduced or abolished menstruation.
[86] weakens resistance to bacteria and is susceptible to skin diseases.
[87] Thus, obesity is a source of various diseases, including adult disease.
[88] Overweight Obesity
[89] One). Hepatic function: There are many functions, but the functions directly related to obesity are metabolic functions such as bile production and the secretion of fat metabolism plasma protein.
[90] * Fat metabolism, bile salts (bile sats): Cholesterol derivatives to emulsify fats to spread to water-soluble intestinal contents. As a result, the fat that enters the small intestine becomes a suspension of millions of small fat particles, helping the digestive enzymes work. Without bile, fat is not digested or absorbed. The diet helps to dissolve cholesterol in the small intestine and cholesterol in the bile. It is reabsorbed into the blood by the ileum, returned to the liver via hepatic portal blood, and newly formed and secreted into bile.
[91] Cholesterol: One of the most important mediators of cholesterol, one of the major causes of obesity, is the bile produced by the liver. Lack of bile salts in the bile reduces cholesterol breakdown, which leads to high blood cholesterol levels and crystallization.
[92] Pancreas: Exocrine glands that secrete digestive enzymes and insulin and glucagon secrete glands that regulate blood glucose metabolism coexist. Insulin is a hormone that lowers blood sugar, while glucagon is a hormone that raises blood sugar. The function of the pancreas has an important relationship with obesity, an organic metabolic relationship with the liver, and a circulatory relationship with the liver about 6-10 times a day, and an indirect circulation relationship with the stomach. Glucose metabolism has a profound relationship with diabetes and with obesity.
[93] Fatal damage to the liver is toxic and liver problems can cause bile problems, and bile problems can cause bile salts. Problems with bile salts can also cause problems with cholesterol disintegration, even with problems breaking down fat into millions of small particles. This is the cause of obesity.
[94] The present invention is mixed with a weight ratio of salt 10 to red pine or Korean native pine Charcoal 90 baked through the digestion process in a vacuum kiln made of flame retardant bricks (500 ℃ ~ 1000 ℃) and then put back into the blast furnace high temperature treatment of 600 ℃ It is characterized by processing into an edible charcoal having a very small pore through and then cooled to powder 325 mesh.
[95] Referring to the manufacturing process of the present invention in detail as follows.
[96] Example 1
[97] Korean Native Pine Charcoal 90% by weight
[98] Salt 10 wt%
[99] The present invention made of the raw material is mixed with 90% by weight of charcoal (charcoal) of red pine or Korean native pine charcoal baked through the digestion process in a vacuum kiln made of refractory bricks, and put it again at high altitude 600 After the high-temperature treatment of ℃ prepared by the edible charcoal having a very small pores and powdered to 325 mesh to prepare the edible charcoal CHA12 of the present invention.
[100] Example 2
[101] Korean native pine charcoal 80% by weight
[102] Salt 10% by weight
[103] 10% by weight of aloe vera powder
[104] The present invention made of the raw material is mixed with the red pine cones baked through the digestion process in a vacuum kiln made of refractory bricks or salt (10% by weight of salt) in 90% by weight of Korean charcoal charcoal (Charcoal) of Korean traditional pine and put again at high altitude 600 After preparing a edible charcoal having a very small pore through the high temperature treatment of ℃ and powdered to 325 mesh and then blended the edible tea of 90% by weight to 10% by weight of aloe powder to prepare the CHA12 in the edible tea of the present invention do.
[105] Example 3
[106] Korean native pine charcoal 75 wt%
[107] Salt 10% by weight
[108] 10% by weight of aloe powder
[109] Bokryeong Powder 5 wt%
[110] The present invention made of the raw material is mixed with the red pine cones baked through the fire extinguishing process in a vacuum kiln made of refractory bricks or 10% by weight of salt (charcoal) of Korean native pine charcoal (Charcoal) and re-added to high altitude 600 After the high-temperature treatment of ℃ prepared by the edible charcoal having a very small pores and powdered into 325 mesh and then mixed with 85% by weight of the edible charcoal Aloe powder 10% by weight bokyeong powder 5% by weight of the edible charcoal of the present invention CHA12 is prepared.
[111] Manufacture process
[112] First process main material
[113] One). Although commercial charcoal used in the market has excellent adsorption power, it is not suitable for edible because of its strong permeability due to oak or mixed wood, which may remain in the human body. Over 20 years of material research, Korean native pine trees are adaptable to humans, are mild and fragrant, can be pulverized with 325mesh, the best technology of powder, and have excellent safety, no negative factors, fusion, decomposition, control of charcoal and salt of Korean pine at high temperature. Since it is the safest adsorbent during the purification process, Korean native pine is the main ingredient.
[114] 2nd process charcoal process
[115] The inner brick (500 ℃ -1000 ℃) is used to make a kiln with a vacuum of 5-10m2 and a height of 2m, and the red pine pine, which is over 10 years old, is cut down and sealed in the kiln. Heat 36 hours to obtain charcoal through digestive vacuum.
[116] Process 3 Edible Charcoal (CHA12) Manufacturing Process
[117] In a blast furnace (600 ℃), charcoal 1ton, 100kg of salt, spread 200kg of charcoal under the blast furnace, sprinkle 20kg of salt, put 200kg of charcoal again, lay 20g of salt on top of it, repeat 5 times and mix 100kg of salt with 1000kg of charcoal. After closing the blast furnace door and resurrecting through high temperature (600 ℃) process to give very small pores, pure edible charcoal (CHA12), the most excellent adsorption detoxification material, is pulverized to 325mesh.
[118] 4th process aloe
[119] After washing and cutting aloe vera clean, put it into a drier, apply heat to 70 ℃ -95 ℃, dry it and grind to 325mesh.
[120] 5th Process
[121] After removing the impurities by washing the Bokryeong, the outer shell is removed and finely pulverized to dry water 325mesh.
[122] 6th process raw materialization
[123] After mixing the edible charcoal (CHA12) powder obtained in the third step with the aloe powder of the fourth step at a mixing rate in the fifth step to obtain a pure edible charcoal (CHA12) material.
[124] Experimental examples of the raw material of the present invention prepared as described above are as follows.
[125] Experimental Example 1 Salmonella Strain Adsorption Test
[126] (One). Enrichment Culture
[127] 1) .General Information (1) Sampling and Handling of Specimens ② Inoculate 1-2 ml of the sample solution prepared by the preparation of the test solution into 10 ml of Selenite F Broth (28) for enrichment liquid, and enrich for 48 hours at 35-37 ℃. Incubated.
[128] (2). Separation Culture
[129] The enriched bacterial solution was transplanted to Desoxycholate Citrate Agar (medium 31) or MacConkey Agar (medium 30), which is a separation medium, and cultured at 35-37 ° C for 24 hours to identify cultures suspected of Salmonella.
[130] (3). Confirmation culture
[131] Select only suspected colonies and lactose non-degrading bacteria from the separation medium, transplant them to agar medium (medium 8), incubate for 18-24 hours at 35-37 ° C, and puncture the cultured cells into TSI agar medium and 37 ± Incubation at 1 ℃ for 18-24 hours to examine the biological properties did not degrade lactose, glucose was broken down so that the medium surface turned yellow. The medium puncture portion that generates gas splits. Hydrogen emulsification was generated and the area near the punctured spot was black.
[132] Morphological test
[133] The isolated bacteria were stained according to the Gram staining method and were Gram-negative bacillus.
[134] Coagulation reaction test
[135] Normally, bacteria were cultured in agar medium using slides to determine the species according to the results of the following Salmonella diagnostic sera.
[136] Ⓐ Salmonella O mixed serum test
[137] The slide aggregation test was performed using O antiserum.
[138] Ⓑ Salmonella O Factor Serum Test
[139] The slide aggregation reaction was examined using group O serum, that is, antiserum of group A, B, C, D and E.
[140] Ⓒ Salmonella H Factor Serum Test
[141] Fungi containing flagella H antigens were tested for in vitro agglutination tests for flagellar antigens a, b, c, d, e, h, G, K, L, r, y.
[142] (4). inspection
[143] After salmonella bacteria 5g or more obtained by the culture experiment as described above, 10g of rice, 50g beef soup (including 1 point of beef, 1 point of shellfish) and 50ml of hot water (20 ℃) were mixed and mixed for 1 hour in a culture glass tube. After storage, the mixture was mixed with 2g of CHA12 and firstly examined by salmonella bacteria extraction method (General Test 7). About 0.5g of Salmonella bacteria were found. In addition, CHA12 single-use (2g) was mixed again and tested again after 30 minutes did not find Salnomella bacteria.
[144] Experimental Example 2 Adsorption experiment of Vibrio parahaemolyticus
[145] (One). Enrichment and Separation
[146] 1) General matters (1) Sampling and handling of samples ② Inoculate 1.0 ml of the sample solution prepared by the preparation of the test solution into peptone water (medium 16) added with 2% Nacl, and incubate at 37 ° C for 18-24 hours, followed by TCBS agar. The medium (medium 17) was plated and incubated at 37 ° C for 18-25 hours.
[147] (2). Identification Law
[148] After confirming the undigested colonies of cyan sucrose with a diameter of 2-4mm on the separation medium, the colonies were estimated and confirmed.
[149] Estimation test
[150] The suspected colonies are taken as platinum and incubated in TSI agar medium (medium 32) on slopes, cavities, LIM medium (medium 18) and ordinary agar medium (medium 8), respectively, at 37 ° C for 24 hours.
[151] Enteric vibrio fermentation of glucose in TSI agar medium (yellow bloated), gas non-produced (bubble unaffected by bubbles, siliceous nondetermined) Lactose, sucrose non-decomposed (red sloped), non-hydrogen sulfide (no buffed black), Lysine Decarboxylase positive (purple ovary), Indole production (red middle layer of reagent), motility positive (cloudy whole opaque), and normal oxidase test by L.A. medium in LIM medium were positive.
[152] Confirmation test
[153] A small amount of the culture medium of TSI or normal agar medium used for the estimation test was taken as platinum wire, and the number of peptones (media 16) added with 0, 3, 8 10% Nacl, VP semi-flow medium (media 19), Purple Broth Base (media 20) ) (1% Mannitol added), Moeller Basal Broth (Medium 21) (1% Arginine added), Moeller Basal Broth (1% Ornithine added), ONPG Broth (Medium 22) and incubated for 4 days at 37 ℃ Incubated for 24 hours at 42 ℃ in Nutrient Broth (Medium 7) to which 3% Nacl was added. Enteritis vibrio was negative for Peptone number with 10% Nacl, negative for development, VP negative, acid production for Mannitol, negative for Ornithine, negative for Arginine degradation, negative for ONPG test, 3 for Peptone number with 3% and 8% Nacl Development was positive at Nutrient Broth with 42% Nacl.
[154] (3). inspection
[155] Rice 50g Beef soup (1 beef clam 1 point) 10g Mix 10g drinking water and mix it with Vibrio parahaemolyticus, put it in a culture tube and store it for 4 hours at 36 ℃, then add 1 bag (2g) to CHA12. After another hour of storage and enteritis vibrio test (General Test 7), enteritis vibriovirus was not detected.
[156] Experimental Example 3 Adsorption Experiment of Bacillus anthracis
[157] One). Emulsion was made with 10 g of beef, and the plain agar medium (medium 8) without salt was plated and plated, and incubated at 37 ° C for 24 hours. It precipitated and developed in Bouillon to form a colony of white-bearing horned vitreous hairs and smeared it so that both ends were cut at right angles as a Gram-positive bacillus and showed a rod-like chain shape. After heating at 80 ° C. for 30 minutes, 0.5-1.0 ml of the guinea pig (250-300 g body weight) was inoculated. Edema occurred at the site of inoculation after 24 hours and died later.
[158] 2). inspection
[159] Isolate and identify the bacteria, add 5.0ml of anthrax, mix 10g of rice 50g beef soup (with 1 point of beef), add 5.0ml of anthrax, add 1 bag (2g) of CHA12 to it, and then mix again After mixing 50 g of drinking water) (20 ° C.), it was proved through an experiment that the anthrax was extracted by anthrax test method (the seventh general test method) as “0” and 2 g of CHA12 adsorbed 5.0 ml of anthrax.
[160] Experimental Example 4 Mycobacterium tuberculosis adsorption experiment
[161] One). More than about 30ml of milk was centrifuged at 3000rpm for 30 minutes, and the holding part was taken in a test tube, and the platinum was taken from the precipitate to make a smear sample and subjected to acidic staining by Ziehl Neelsen method and examined. Equivalent amount of 8% NaOH solution was added to the holding part, and about 10% of 4% NaOH solution was added to the precipitate, and the mixture was mixed well. 0.1 ml of each was added dropwise to 3% Okawa medium (Medium 24), and the medium was incubated at 37 ° C. After lying on the side and waiting for most samples to be absorbed, the test tube of the medium was kept tight and culture was continued for 2 months, and the occurrence of bacterial colonies was occasionally observed. After incubation, the above sample was added dropwise with hydrochloric acid solution to which BTB was added, and then inoculated into the guinea pig's skin 1-2 ml each after neutralization. The guinea pig used here was a tuberculin-responsive negative body weight of 300g or more and occasionally caused tuberculin reaction from 2 weeks after inoculation. From 3 weeks, she showed positive reaction, gradually decreased body weight, induration or ulceration at the inoculation site, and local lymph node swelling. After 4-8 weeks, guinea pigs were killed and necropsied, and the tuberculous changes of lymph nodes and organs were observed. The organs of the lesions were aseptically collected and cultured in 1% Okawa medium to identify TB bacteria.
[162] 2). inspection
[163] 50g of guiinea pig organs, and then 50g of rice, 1g of beef soup (1 point of clam) 10g of hot water (20 ℃) CHA12 2g mixed mixer and kept at about 30 ℃ for 1 hour after the tuberculosis test 7 test, but did not find the tuberculosis bacteria. After the second examination, no tuberculosis bacteria were found.
[164] Experimental Example 5 Brucella Bacteria Adsorption Experiment
[165] One). 30 ml of milk was centrifuged at 3000 rpm for 30 minutes to directly incubate the holding part and sediment by the following incubation method, and three mice (12-15 g) intraperitoneally with 3-5 ml of three guinea pigs (250-300 g body weight). 0.25-0.5ml was injected subcutaneously. The emulsion was filtered with sterile gauze and then the filtrate or the supernatant obtained by centrifugation at 1000 rpm for 5 minutes was inoculated into the experimental animals. The sample was contaminated by various bacteria and added to the gentian biolet corresponding to one hundred thousandth of its weight to Liver agar, and incubated at 37 ° C. under 10% carbon dioxide for 5 days. The colonies formed showed a small round, somewhat raised, transparent color and not colored. When stained and examined, it looked like cocci as Gram-negative monobacterium. Incubated at 37 ° C. for 24 hours at Bouillon, the fungus grew cloudy, and after 10 days, the cloud became more turbid and reddish fungi were agglomerated from the surface to the tube wall like a biofilm. The fungus had no motility and almost no degradation of saccharides. Negative Indole, MR and VP reactions were negative. Injected into the experimental animals were serologically diagnosed whether the antibody against the bacteria was formed in the serum of the experimental animals three weeks after the inoculation, and cultured the main bacteria in the spleen.
[166] 2). inspection
[167] 50g (1 beef clam 1 point) 10g drinking water 50g (20 ℃) of the spleen and rice 50g of the above laboratory animals with Brucella bacteria, and then mixed and mixed for 1 hour (30 ℃) in a culture glass bottle After mixing 2 g of CHA12, Brucella was not tested positive by Brucella test (General Test 7). The second test was the same.
[168] Experimental Example 6 Staphylococcus aureus adsorption experiment
[169] (One). Enrichment Culture
[170] One). General (1) Sampling and handling of samples ② 1 ml of the sample solution prepared by the preparation of the test solution was inoculated into Tryptic Soy Broth (Medium 23) containing 10% Nacl and enriched for 16 hours at 35-37 ℃.
[171] (2). Separation Culture
[172] The enriched bacterial solution was plated in yolk-added mannitol saline agar medium (medium 14) and incubated at 37 ° C. for 20 hours. As a result of culture, yellow opaque colonies (mannitol decomposition) were observed in egg yolk-added mannitol agar medium, and colonies with turbid white rings (positive yolk reactions) around colonies were identified and tested according to the following.
[173] (3). Test
[174] Colonies on isolated culture medium were transferred to normal agar medium (medium 8), incubated at 37 ° C. for 24 hours, and then Gram stained to identify Gram-positive cocci with staphylococci. Gram-positive cocci with staphylococci were identified aseptically by 0.5-1m in a test tube sterilized with sterile physiological saline with coagulase test and rabbit serum (5% fresh blood). Bacillus inoculated directly or incubated pure in normal agar medium inoculated and incubated at 37 ℃. Coagulation or fibrin precipitation was determined to be coagulase positive at any time after 3, 6, and 24 hours of incubation, and coagulase-positive bacteria were tested with coagulase-positive bacteria and negative control bacteria. The blood was collected at a ratio of 4 blood doses to 1 dose of 5% sodium citrate solution sterilized in healthy rabbits, and immediately centrifuged at 1,500 rpm for 10 minutes to aseptically isolate.
[175] (4). inspection
[176] Rice 50g Beef soup (1 beef clam 1 point) 10g and 50ml of hot water (20 ℃), and then inoculated with the incubated Staphylococcus aureus inoculated in the culture glass tube and stored for 4 hours (30 ℃). After putting 2g of CHA12 into the specimen, it was stored for another hour (30 ℃) and tested for staphylococcus. The test result was negative.
[177] Experimental Example 7 Residual Pesticide Adsorption Experiment
[178] EPN, Diazinon, Dimethoate, Malathion, Parathion, Phenythrothione, Pention, Pendoate, Methidation, Azinfosmethyl, Ometoate
[179] device
[180] Gas chromatograph: nitrogen, phosphorus detector (NPD) or salt light detector was used.
[181] Reagent
[182] * Water: Distilled water
[183] * Amberlite XAD-8 resin: After swelling Amberlite XAD-8 in methanol, 2N ammonia water.Methanol (1: 9) mixture water 2N hydrochloric acid.Methanol (1: 1) mixture and water Rinse with water until neutral
[184] * Standard stock solution: Dissolve each organophosphate in nucleic acid to make 100mg / kg
[185] * Standard solution: Dissolve the standard stock solution in hexane, mix and dilute to appropriate concentration.
[186] * Other reagents: 3) Multi-component test method (1) Organic chlorine agent ②According to the reagent
[187] Preparation of test solution
[188] Ⓐ Extraction
[189] 3) Multi-component test method (1) Organic chlorine ③ Test solution preparation ⓐ Test up to * by extraction, and then follow the operation below. Transfer the filtrate to a separatory funnel with 400 ml of 5% sodium chloride solution in advance, add 100 ml of 20% dichloromethane-containing benzene, shake it vigorously for 1 minute, and stop. Add 100 ml of benzene and repeat as above. Combine the dichloromentane and benzene layers with the separatory funnel and wash them with 100 ml of water. The dichloromethane and benzene layers are passed through anhydrous sodium sulfate column and dehydrated. The solvent was blown off under reduced pressure on a water bath below ° C, and the residue was dissolved in 5 ml of hexane.
[190] Ⓑ Sample
[191] Add 1 apple to the EPN, Diazinon, Dimethate, Malathion, Parathion, Phenythrothione, Pention, Pendoate, Methidathion, Azinphosmethyl, Ometoate mixed solution for about 1 hour, and then take out and mix Take a 100g sample, mix 2g of 1 bag of CHA12, and make it as a sample. In a column tube with a diameter of 15mm and a length of 30mm, 5g of a mixture of activated carbon and microcrystalline cellulose powder (1:10), and about 5g of anhydrous sodium sulfate are suspended in benzene, respectively. After filling, the solution was poured out to the extent that a small amount of benzene remained on the top, and the above concentrated solution was added to this column, eluted with 150 ml of benzene, and the eluate was almost blown off under reduced pressure in a 40 ° C water bath. After completely blowing off the residue was dissolved in acetone to make exactly 5ml to make a test solution.
[192] Test operation
[193] Measurement conditions of gas chromatography
[194] Column filler
[195] Fixed carriers: Chromosolve W (AW-DMCS) for Chromatography, Chlomosolve G (AW-DMCS) and Gas Chromium Q (80-100 mesh) or equivalent.
[196] Stationary Liquids: 4% OV-101, 10% DC-200, 10% OF-1, 5% OV-210 and 5% OV-225
[197] Column: glass tube with a diameter of 2-3 mm and a length of 100-200 cm
[198] Inlet and detector temperature: 180-270 ° C depending on column temperature
[199] Column temperature: elevated temperature-initial temperature 140 ℃ After the test solution was injected, the temperature was raised at a rate of 4 ℃ / min and maintained until the last peak at 240 ℃.
[200] Constant temperature condition -160-240 ℃
[201] Carrier gas and flow rate: nitrogen, 30-50ml / min
[202] Qualitative test: 3) Multi-component test method (1) Organic chlorine agent ④ Test operation The procedure was according to the qualitative test.
[203] Quantitative test: 3) Multicomponent test method (1) Organic chlorine agent ④ Test procedure Followed by quantitative test.
[204] (4). inspection
[205] As a result of the test, a small amount of mixed pesticides was detected. After 4 hours of mixing and mixing the ingredients with 50ml CHA12 2g of distilled water, no pesticides were detected and the result was the same.
[206] Experimental Example 8 Non-Adsorption Bifiddobacterium
[207] After mixing 1g of sample Bifidobacteria and 1g of CHA12
[208] Mix the above mixture to 100ml by adding 10% skim milk powder dilute solution or physiological saline, and homogenize by mixing in a mixer.
[209] Diluted solution was added to 1 ml of the sample solution (10-2 solution) of ① to make 10ml, and then 10-4, 10-5, 10-6, and 10-7 samples were prepared in the same manner.
[210] Inoculate 0.05 ml of each diluted test solution onto BL agar medium (medium 15) and apply it with sterile candle bar.
[211] Put the sterile petri dish in an anaerobic box and incubated for 48-72 hours at 37 °, and measured the colony count after incubation, and multiplied by the dilution factor (× 20) to calculate the number of viable bacteria per sample. However, only diluted samples of 30 to 300 colonies were measured per plate.
[212] Growth of bacteria on BL agar plate after culture
[213] Bifidobacterium longum: A brownish-brownish brown hemispherical ridge formed a colony of about 1.0-2.0 mm in diameter with a reddish brown in the center.
[214] * Bifidobacterium bifidum: Milky brown-grey bulge centered reddish brown, about 0.5-1.5mm in diameter.
[215] * Bifidobacterium breve: Milky white-brownish hemispherical, rounded colony of 1.0-2.0mm in diameter with raised center.
[216] From the above results, it was confirmed that CHA12 did not adsorb beneficial bacteria.
[217] Experimental Example 9 Arsenic Adsorption Experiment
[218] (One). reagent
[219] One). Silver diethyldithiocaamic acid pyridine solution
[220] 1 g of diethyldithiocaamic acid is dissolved in 200 ml of pyridine. Shade it and store it in a cool dark place
[221] 2). Zinc (arsenic): Soak 20-30 mesh of zinc in 1% copper sulfate solution until black, rinse with water and dry.
[222] 3). Tin chloride solution
[223] Dissolve 4 g of tin 1 in 125 ml of hydrochloric acid, add 250 ml of water, and store it in a static bottle.
[224] (2). Device
[225] A: Color Flask (Contents 100-125ml)
[226] B: absorption tube (lead acetate glass wool)
[227] C: Gas guide pipe (inner diameter 2, outlet 0.5)
[228] D: Absorber
[229] (3). Test solution
[230] Rice 50g Beef Ripe 10g
[231] Mix 2 g of purified water 50ml CHA12 and use it as a test solution.
[232] (4). Trial operation
[233] Take 25 ml of the test solution into a color flask, add 1 drop of bromine phenol blue solution, neutralize with ammonia water, add water to make 25 ml, add 5 ml of hydrochloric acid (1 + 1), 2 ml of potassium iodide solution, and 5 ml of tin chloride solution at room temperature. Leave for 15 minutes, add 3 ml of diethyldithiocaamic acid pyridine solution to the absorber, add 3 g of zinc to the color development flask, and immediately connect the absorber and gas induction pipes. After adjusting the bubble to be small and continuous, let it stand at 20-25 ℃ for 1 hour, then loosen the device and mix the liquid attached to the inner wall of the gas induction pipe well with the liquid in the absorber. The diethyldithiocarbamic acid was measured for absorbance near the wavelength of 525 nm using pyridine solution as a control solution, and separately 0.0, 2.0, 4.0, 6.0, 8.0, and 10.0 ml of the arsenic acid standard solution. By taking this test solution, and non-small bars obtained from the prepared calibration curve, the content of arsenic and subjected to the blank test solution was the same amount of measuring the absorbance of each operation and then as a test solution was not detected.
[234] Experimental Example 10 Mercury Adsorption Experiment
[235] (One). reagent
[236] One). Tin chloride solution: 10 g of tin chloride is dissolved in 0.5 N sulfuric acid to make 1000 ml.
[237] 2). Mercury standard solution: Dissolve 0.135 g of mercuric chloride in 10% and 100 ml of nitric acid, and add water to make 1000 ml. When using, dilute this solution 1000 times with 1% nitric acid to make standard solution.
[238] Mercury standard solution 1ml = 0.1 microL Hg
[239] (2). Test solution
[240] Rice 50g Beef 10g ripened water, 50ml CHA12 2g mixed mixer to test solution
[241] (3). Trial operation
[242] Adjust test solution and blank test solution to 20% (V / V) sulfuric acid concentration, take each 100ml test solution bottle, connect to reducing gasifier, add 10ml of the first tin chloride solution, and immediately stop plug and air by diaphragm pump. Circulate in the absorption cell and measure the absorbance at wavelength 253.7nm, add 100ml of mercury standard solution to water, make 100ml, and perform the same operation as the test solution. When mercury was determined, no mercury was detected.
[243] Experimental Example 11 Heavy Metal Adsorption Experiment
[244] (One). reagent
[245] One). Lead standard solution: 0.1598 g of lead nitrate is dissolved in nitric acid (2.5-> 100) to make 100 ml, and then diluted to 100 or 1000 times with nitric acid (1-> 100).
[246] (2). Test solution
[247] Rice 50g Beef 10g ripened water, 50ml CHA12 2g mixed mixer to test solution
[248] (3). Test: Take 20 ml of the test solution into the color tube and add 1, 2, 3 ..... 10 ml of lead standard solution to the color tube separately, neutralize with aqueous ammonia, add 50 ml of 2% 5% acetic acid and water, and then sodium sulfide. Add 2 drops of solution, mix well, leave for 5 minutes, and color the white to find the heavy metal content. No heavy metal was detected.
[249] Experimental Example 12 Alcohol Adsorption Experiment
[250] 100 ml of alcohol was added to 2 g of CHA12, and the sample was placed in a 500 ml distillation bottle, and 25 ml of distilled water was added. After transfer to the cylinder and tried using the main flatness at 15 ℃ all the alcohol was adsorbed.
[251] Experimental Example 13 Methanol Adsorption Experiment
[252] (One). Methanol
[253] One). Fuchsin sulfite
[254] Reagent: Potassium permanganate solution: Add 75 ml of phosphoric acid to water to make 500 ml, and dissolve 15 g of potassium permanganate.
[255] Aquatic solution: Cool sulfuric acid by adding the same amount of water, and dissolve 25g of aquatic acid in 500ml.
[256] Fusulfite solution: Dissolve 0.5 g of basic fuxin in 300 ml of boiling water, cool, dissolve 5 g of anhydrous sodium sulfate in 50 ml of water, mix the two solutions, add 5 ml of hydrochloric acid, and dilute this mixture with water to make 500 ml. It was used after leaving for 5 hours. This solution is placed in a brown bottle and stored in a cool dark place.
[257] 2). exam
[258] 100 ml of CHA12 was added and distilled to give 100 ml of the emulsion, 40 ml of water was added to 10 ml of the emulsion, and 5 ml of this sample and methanol color standard were added to the same test tube. After adding potassium permanganate to decolorize and completely decolorizing, add 5 ml of fusulfite solution to each test tube, shake well, and leave it at room temperature for 30 minutes. Then, compare the color of the sample solution with the color of the standard solution at 585 nm. When the absorbance was measured to determine the content of methane in the sample, methanol could not be obtained.
[259] As described above, the present invention is used as a main ingredient of health foods to remove toxic components or harmful bacteria in the body during digestion, which prevents food poisoning, promotes digestion, maintains health, and restores normal human function.
权利要求:
Claims (3)
[1" claim-type="Currently amended] 90kg% of red pine or Korean native pine charcoal is mixed with 10% by weight of salt, put it in the blast furnace, close the door, and make it as an edible charcoal with very small pores through high temperature treatment at 600 ℃. Method for producing an edible charcoal (CHA12) using pine charcoal, characterized in that the pulverized into a mesh to produce a main raw material of health food.
[2" claim-type="Currently amended] 90kg% of red pine or Korean native pine charcoal is mixed with 10% by weight of salt, put it in the blast furnace, close the door, and make it as an edible charcoal with very small pores through high temperature treatment at 600 ℃. Grinding by a mesh to prepare the edible charcoal (CHA12) using pine charcoal, characterized in that by mixing 10% by weight of aloe powder to 90% by weight of the edible charcoal to prepare a main raw material of health food.
[3" claim-type="Currently amended] 90kg% of red pine or Korean native pine charcoal is mixed with 10% by weight of salt, put it in the blast furnace, close the door, and make it as an edible charcoal with very small pores through high temperature treatment at 600 ℃. Crushed into a mesh to prepare the edible charcoal (CHA12) using pine charcoal, characterized in that to prepare the edible charcoal mixed with 85% by weight of aloe powder 10% by weight, Bokryeong powder 5% by weight as a raw material of health food.
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同族专利:
公开号 | 公开日
KR100457821B1|2004-11-18|
引用文献:
公开号 | 申请日 | 公开日 | 申请人 | 专利标题
法律状态:
2001-06-08|Application filed by 차순옥
2001-06-08|Priority to KR10-2001-0032187A
2002-12-16|Publication of KR20020093432A
2004-11-18|Application granted
2004-11-18|Publication of KR100457821B1
优先权:
申请号 | 申请日 | 专利标题
KR10-2001-0032187A|KR100457821B1|2001-06-08|2001-06-08|The manufacturing process of edible charcoal using pine charcoal|
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